Crucible in very hot electric (arc) furnace

QUESTION:

Trying to obtain a source of very high temperature (above 1500oC) I tried a welder with carbon rods connected on pieces of coal in a refractory cilindrical hole of 5 cm diameter. The coal gets white hot (too bright to be viewed by the naked eye) while the welder (100 Amps) hums. So the temperature is not the problem. But I want to melt platinum class metals this way *without* being contaminated by the carbon. Hessian crucibles break apart (cannot withstand such temps ?). Any ideas ?

ANSWER:

It's not my field, we have Mo wire furnace (1700C), and Lindberg 3 zone 1200C tube furnace, where we use refractory tubes with vacuum or gas pressure, but we really are only interested in major composition changes of materials within the tubes. I'd talk to some of the tube furnace manfacturers
( such as Lindberg), and some of the refractory tube suppliers
( who should be available on the WWW ).


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